INSTRUMENT CONTROL PARAMETERS: Agilent GC_Only ------------------------------------------------- D:\MassHunter\GCMS\1\methods\FID_NDA206316.M Fri May 09 11:16:30 2014 Control Information ------- ----------- Sample Inlet : GC Injection Source : GC ALS No Sample Prep method has been assigned to this method. Oven Equilibration Time 3 min Max Temperature 240 degrees C Slow Fan Disabled Oven Program On 80 °C for 0 min #1 then 10 °C/min to 120 °C for 9 min #2 then 40 °C/min to 220 °C for 5 min Run Time 20.5 min QQQ Collision Cell EPC He Quench Gas On 2.25 mL/min N2 Collision Gas On 1.5 mL/min Front Injector Syringe Size 10 μL Injection Volume 5 μL Solvent A Washes (PreInj) 2 Solvent A Washes (PostInj) 0 Solvent A Volume 8 μL Solvent B Washes (PreInj) 2 Solvent B Washes (PostInj) 0 Solvent B Volume 8 μL Sample Washes 1 Sample Wash Volume 8 μL Sample Pumps 2 Dwell Time (PreInj) 0 min Dwell Time (PostInj) 0 min Solvent Wash Draw Speed 300 μL/min Solvent Wash Dispense Speed 6000 μL/min Sample Wash Draw Speed 300 μL/min Sample Wash Dispense Speed 6000 μL/min Injection Dispense Speed 6000 μL/min Viscosity Delay 1 sec Sample Depth Disabled Injection Type Standard L1 Airgap 0.2 μL Sample Overlap Sample overlap is not enabled Front MM Inlet He Mode Split Heater On 220 °C Pressure On 9.2855 psi Total Flow On 122.37 mL/min Septum Purge Flow On 3 mL/min Temperature Program On 220 °C for 0 min Run Time 20.5 min Gas Saver On 15 mL/min After 2 min Split Ratio 5 :1 Split Flow 99.476 mL/min Cryo Off Back COC Inlet He ***Excluded from Affecting GC's Readiness State*** Mode Track Oven Pressure Off Septum Purge Flow On 15 mL/min Thermal Aux 2 (MSD Transfer Line) Heater On Temperature Program On 250 °C for 0 min Run Time 20.5 min Column #1 J&W 125-0232DB-210 %0% Trifluopropylsilox 240 °C: 30 m x 530 μm x 1 μm In: Front MM Inlet He Out: Vacuum (Initial) 80 °C Pressure 9.2855 psi Flow 19.895 mL/min Average Velocity 164.88 cm/sec Holdup Time 0.30324 min Flow Program On 19.895 mL/min for 0 min Run Time 20.5 min Front Detector FID ***Excluded from Affecting GC's Readiness State*** Heater On 250 °C H2 Flow On 30 mL/min Air Flow On 400 mL/min Makeup Flow Off Const Col + Makeup Off Flame On Electrometer On Valve 1 Other Off PCM A-1 N2 ***Excluded from Affecting GC's Readiness State*** Pressure Program Off 10 psi for 0 min Run Time 20.5 min PCM A-2 N2 ***Excluded from Affecting GC's Readiness State*** Pressure Program Off 10 psi for 0 min Run Time 20.5 min Signals Signal #1: Front Signal Save On 50 Hz Signal #2: Test Plot Save Off 50 Hz Signal #3: Test Plot Save Off 50 Hz Signal #4: Test Plot Save Off 50 Hz END OF INSTRUMENT CONTROL PARAMETERS ------------------------------------